1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane

Base Information

• Chemical Name: 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane
• CAS No.: 82247-15-2
• Molecular Formula: C₃₂H₃₀O₅
• Molecular Weight: 494.587

Synonyms:1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane

Chemical Property of 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane

Chemical Property:

Purity/Quality:

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Technology Process of 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane

There total 4 articles about 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

threo-1-(3,4-Dimethoxyphenyl)-1-(9,10-dihydroxyanthracen-10-yl)-2-(2-methoxyphenoxy)propane (84064-72-2) → threo-10,11-Dihydro-2,3-dimethoxy-11-<1-(2-methoxyphenoxy)ethyl>-5,10-o-benzeno-5H-dibenzocyclohepten-10-ol (84064-73-3) + 10-[(1S,2S)-1-(3,4-Dimethoxy-phenyl)-2-(2-methoxy-phenoxy)-propyl]-10H-anthracen-9-one (82247-15-2,86956-00-5)

Guidance literature:

With boron trifluoride diethyl etherate; In acetic acid; for 24h; Ambient temperature;

DOI:10.1021/jo00151a018

Reference yield:

9-anthrol trimethylsilyl ether (28871-54-7) + 1-bromo-1-(3,4-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane (86956-05-0,86956-06-1) → chloro-trimethyl-silane (75-77-4) + anthracen-9(10H)-one (90-44-8) + 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane (82247-15-2) + 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane (82247-15-2,86956-00-5)

Guidance literature:

With zinc dibromide; In chloroform-d1; for 0.0333333h; Further byproducts given; NMR-tube;

DOI:10.1021/jo00170a003

Reference yield:

9-anthrol trimethylsilyl ether (28871-54-7) + 1-bromo-1-(3,4-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane (86956-05-0,86956-06-1) → chloro-trimethyl-silane (75-77-4) + anthracen-9(10H)-one (90-44-8) + 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane (82247-15-2) + 1-(3,4-dimethoxyphenyl)-1-(9,10-dihydro-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)propane (82247-15-2,86956-00-5)

Guidance literature:

With zinc dibromide; In chloroform-d1; for 0.0333333h; Further byproducts given; NMR-tube;

DOI:10.1021/jo00170a003

upstream raw materials:

9-anthrol trimethylsilyl ether

1-bromo-1-(3,4-dimethoxyphenyl)-2-(2-methoxyphenoxy)propane

threo-1-(3,4-Dimethoxyphenyl)-1-(9,10-dihydroxyanthracen-10-yl)-2-(2-methoxyphenoxy)propane

10-[(1S,2S)-1-(3,4-Dimethoxy-phenyl)-2-(2-methoxy-phenoxy)-propyl]-10-hydroxy-10H-anthracen-9-one

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