Trityl-L-Phenylalanine diethylammonium salt

Base Information

• Chemical Name: Trityl-L-Phenylalanine diethylammonium salt
• CAS No.: 3226-92-4
• Molecular Formula: C28H25NO2.C4H11N
• Molecular Weight: 480.65
• Hs Code.: 2922499990
• Mol file: 3226-92-4.mol

Synonyms:diethylammonium (S)-3-phenyl-2-(tritylamino)propanoate

Chemical Property of Trityl-L-Phenylalanine diethylammonium salt

Chemical Property:

• PSA: 61.36000
• LogP: 6.66160
• Storage Temp.: Store at 0°C

Purity/Quality:

99% ^*data from raw suppliers

TRT-PHE-OH ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Trityl-L-Phenylalanine diethylammonium salt

There total 2 articles about Trityl-L-Phenylalanine diethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6) + trityl chloride (76-83-5) + diethylamine (109-89-7) → Trt-Phe*Et2NH (3226-92-4,273747-93-6)

Guidance literature:

Yield given. Multistep reaction;

Reference yield:

N,O-bis(trimethylsilyl)phenylalanine (7364-51-4) + trityl chloride (76-83-5) + diethylamine (109-89-7) → Trt-Phe*Et2NH (3226-92-4,273747-93-6)

Guidance literature:

Yield given. Multistep reaction; 1.) CHCl₃, 1 h, reflux;

Reference yield:

Trt-Phe*Et2NH (3226-92-4,273747-93-6) → triphenylmethane (519-73-3) + L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6)

Guidance literature:

With magnesium iodide; In tetrahydrofuran-d8; at 120 ℃; for 2h; Overall yield = > 95 %Spectr.; chemoselective reaction; Inert atmosphere; Microwave irradiation;

DOI:10.1002/chem.201501799

upstream raw materials:

L-phenylalanine

trityl chloride

diethylamine

N,O-bis(trimethylsilyl)phenylalanine

Downstream raw materials:

triphenylmethane

L-phenylalanine

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