(R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide

Base Information

Chemical Name:(R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide
CAS No.:853570-32-8
Molecular Formula:C₁₈H₂₉NO₄S
Molecular Weight:355.499
Hs Code.:

Synonyms:(R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide

Chemical Property:

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Technology Process of (R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide

There total 5 articles about (R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 853570-31-7
ethyl 7-hydroxy-8-(p-tolylsulfinyl)nonanoate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 853570-32-8
(R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide

Guidance literature:: With trimethylaluminum; In dichloromethane; toluene; Heating;
DOI:10.1021/ol050620a

Reference yield:

: 853570-30-6
ethyl 7-oxo-8-(p-tolylsulfinyl)nonanoate

: 853570-32-8
(R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: DIBALH; ZnBr₂ / tetrahydrofuran; heptane / 2 h / -78 °C

2: 70 percent / AlMe₃ / CH₂Cl₂; toluene / Heating

With trimethylaluminum; diisobutylaluminium hydride; zinc dibromide; In tetrahydrofuran; n-heptane; dichloromethane; toluene;
DOI:10.1021/ol050620a

Reference yield:

: 2050-20-6
diethyl pimelate

: 853570-32-8
(R)-7-Hydroxy-8-((R)-toluene-4-sulfinyl)-nonanoic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: LDA / tetrahydrofuran / -78 - 0 °C

2: DIBALH; ZnBr₂ / tetrahydrofuran; heptane / 2 h / -78 °C

3: 70 percent / AlMe₃ / CH₂Cl₂; toluene / Heating

With trimethylaluminum; diisobutylaluminium hydride; zinc dibromide; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; dichloromethane; toluene;
DOI:10.1021/ol050620a