Technology Process of C23H13BrCl2N4O3S
There total 10 articles about C23H13BrCl2N4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuryl dichloride;
In
dichloromethane;
at 0 ℃;
for 1.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 6 h / 170 °C / Heating / reflux
2: Monoperoxyphthalic acid, magnesium salt / methanol; dichloromethane / 1 h / 0 °C
3: sodium acetate / 5 h / Heating / reflux
4: Monoperoxyphthalic acid, magnesium salt / methanol; dichloromethane / 2 h / 0 - 20 °C
5: methanol; sodium hydroxide; water / tetrahydrofuran / 1.5 h / 0 °C
6: sulfuryl dichloride / dichloromethane / 1.5 h / 0 °C
With
methanol; sodium hydroxide; sulfuryl dichloride; water; sodium acetate; Monoperoxyphthalic acid, magnesium salt;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Monoperoxyphthalic acid, magnesium salt / methanol; dichloromethane / 1 h / 0 °C
2: sodium acetate / 5 h / Heating / reflux
3: Monoperoxyphthalic acid, magnesium salt / methanol; dichloromethane / 2 h / 0 - 20 °C
4: methanol; sodium hydroxide; water / tetrahydrofuran / 1.5 h / 0 °C
5: sulfuryl dichloride / dichloromethane / 1.5 h / 0 °C
With
methanol; sodium hydroxide; sulfuryl dichloride; water; sodium acetate; Monoperoxyphthalic acid, magnesium salt;
In
tetrahydrofuran; methanol; dichloromethane;