(2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone

Base Information

Chemical Name:(2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone
CAS No.:220018-34-8
Molecular Formula:C₁₆H₂₈O₃SSi
Molecular Weight:328.548
Hs Code.:

Synonyms:(2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone

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Technology Process of (2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone

There total 6 articles about (2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 189223-93-6
C₁₆H₂₈OSSi

: 220018-34-8
(2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/ja0691728

Reference yield: 93.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 220018-33-7
(2R)-2-methyl-3-(phenylsulfonyl)propan-1-ol

: 220018-34-8
(2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 17h; Ambient temperature;
DOI:10.1039/a805856c

Reference yield:

: 101212-36-6
(R)-(-)-2-methyl-3-(phenylthio)propan-1-ol

: 220018-34-8
(2R)-3-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-methylpropyl phenyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / imidazol / tetrahydrofuran / 12 h / 20 °C

2: 99 percent / NaHCO₃; mCPBA / CH₂Cl₂ / 5 h / 20 °C

With 1H-imidazole; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja0691728