ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide

Base Information

Chemical Name:ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide
CAS No.:878488-05-2
Molecular Formula:C₆H₁₂N₂O₇*H₃N
Molecular Weight:241.201
Hs Code.:

Synonyms:ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide

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Chemical Property of ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide

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Technology Process of ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide

There total 1 articles about ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 57820-45-8
1-Desoxy-N-hydroxy-β-D-glucopyranosylamin

: 492-61-5
β-D-glucose

: 492-62-6
alpha-D-glucopyranose

: 878488-05-2
ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide

: 57820-48-1
(E)-D-glucose oxime

Guidance literature:: 1-Desoxy-N-hydroxy-β-D-glucopyranosylamin; With hydrogenchloride; sodium nitrite; at 0 ℃; for 1h;

With ammonium hydroxide; Further stages. Further byproducts.;
DOI:10.1002/chem.200500325

Reference yield: 56.0%

: 878488-05-2
ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide

: 98-88-4
benzoyl chloride

: 77-78-1
dimethyl sulfate

: 878488-07-4
N-methoxy-N-nitroso-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosylamine

: 878488-06-3
(Z)-1-methoxy-2-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)diazene-2-oxide

Guidance literature:: ammonium 2-(β-D-glucopyranosyl)diazene-1-olate-2-oxide; dimethyl sulfate; With sodium hydrogencarbonate; In water; at 23 ℃; for 24h;

benzoyl chloride; With pyridine; at 5 ℃; for 24h; Further stages.;
DOI:10.1002/chem.200500325