2,4-Mesitylenedisulfonyl Dichloride

Base Information

• Chemical Name: 2,4-Mesitylenedisulfonyl Dichloride
• CAS No.: 68985-08-0
• Molecular Formula: C9H10Cl2O4S2
• Molecular Weight: 317.214
• Hs Code.: 29309090
• European Community (EC) Number: 633-276-1
• DSSTox Substance ID: DTXSID00394370
• Nikkaji Number: J837.735I
• Wikidata: Q72488777
• Mol file: 68985-08-0.mol

Synonyms:68985-08-0;2,4-Mesitylenedisulfonyl Dichloride;2,4,6-Trimethylbenzene-1,3-disulfonyl dichloride;2,4,6-trimethylbenzene-1,3-disulfonyl Chloride;1,3-Benzenedisulfonyldichloride, 2,4,6-trimethyl-;2,4,6-Trimethyl-1,3-benzenedisulfonyl Dichloride;2,4,6-Trimethylbenzene-1,3-disulfonyldichloride;SCHEMBL2263745;DTXSID00394370;LNXKRGBQKLXFTB-UHFFFAOYSA-N;MFCD00009796;2,4-Mesitylenebis(sulfonyl chloride);AKOS015840495;CS-W012023;GS-5560;2,4-MESITYLENEDISULFONYL CHLORIDE;FT-0641216;M1186;REF DUPL?2,4-Mesitylenedisulfonyl Dichloride;H10526;J-507258

Chemical Property of 2,4-Mesitylenedisulfonyl Dichloride

Chemical Property:

• Vapor Pressure: 3.89E-07mmHg at 25°C
• Melting Point: 125 °C
• Refractive Index: 1.555
• Boiling Point: 428.1 °C at 760 mmHg
• Flash Point: 212.7 °C
• PSA: 85.04000
• Density: 1.499 g/cm³
• LogP: 4.62840
• Solubility.: soluble in Toluene
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 315.9397565
• Heavy Atom Count: 17
• Complexity: 430

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,4-Mesitylenedisulfonyl Dichloride ^*data from reagent suppliers

Safty Information:

• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1S(=O)(=O)Cl)C)S(=O)(=O)Cl)C

Technology Process of 2,4-Mesitylenedisulfonyl Dichloride

There total 5 articles about 2,4-Mesitylenedisulfonyl Dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1,3,5-trimethyl-benzene (108-67-8) → 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride (68985-08-0)

Guidance literature:

With chlorosulfonic acid; 1.) -5 deg C, 1h, 2.) RT, 3h;

DOI:10.1016/S0040-4020(01)96778-X

Reference yield:

2,4,6-trimethylbenzene-1-sulfonyl fluoride (384-98-5) → 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride (68985-08-0)

Guidance literature:

With chlorosulfonic acid; at 20 ℃;

Reference yield:

chlorosulfonic acid (7790-94-5) + 2,4,6-trimethylbenzene-1-sulfonyl fluoride (384-98-5) → 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride (68985-08-0)

Guidance literature:

at 20 ℃;

upstream raw materials:

2,4,6-trimethylbenzene-1-sulfonyl fluoride

1,3,5-trimethyl-benzene

chlorosulfonic acid

sulfuryl dichloride

Downstream raw materials:

1,2-di-p-tolylethane

1,2-bis(4-methoxyphenyl)ethane

1,2-bis(3-methoxyphenyl)ethane

1,2-bis(thiophen-2-yl)ethane

Refernces