phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

Base Information

Chemical Name:phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate
CAS No.:1419604-29-7
Molecular Formula:C₂₁H₂₇N₃O₅
Molecular Weight:401.462
Hs Code.:

Synonyms:phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

Suppliers and Price of phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

There total 7 articles about phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1419604-27-5
phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

: 1419604-29-7
phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 23 ℃; for 1h;

Reference yield:

: 55338-73-3
5-amino-2-cyanopyridine

: 1419604-29-7
phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 - 23 °C

2: diisobutylaluminium hydride / tetrahydrofuran; toluene / 3 h / -78 °C

3: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 3 h / 0 - 23 °C

4: sulfuric acid / 3 h / 50 °C

5: pyridine / acetone / 1 h / 0 - 23 °C

6: triethylamine / dichloromethane / 1 h / 0 - 23 °C

With pyridine; sulfuric acid; sodium tris(acetoxy)borohydride; sodium hydride; diisobutylaluminium hydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 1419604-19-5
5-(dibenzylamino)picolinonitrile

: 1419604-29-7
phenyl 6-((2-methoxyethyl-N-tert-butoxycarbonyl-amino)methyl)pyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 3 h / -78 °C

2: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 3 h / 0 - 23 °C

3: sulfuric acid / 3 h / 50 °C

4: pyridine / acetone / 1 h / 0 - 23 °C

5: triethylamine / dichloromethane / 1 h / 0 - 23 °C

With pyridine; sulfuric acid; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; acetone; toluene;