phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

Base Information

Chemical Name:phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate
CAS No.:1419604-27-5
Molecular Formula:C₁₆H₁₉N₃O₃
Molecular Weight:301.345
Hs Code.:
Mol file:1419604-27-5.mol

Synonyms:phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

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Chemical Property of phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

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Technology Process of phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

There total 5 articles about phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1419604-25-3
6-((2-methoxyethylamino)methyl)pyridin-3-amine

: 1885-14-9
phenyl chloroformate

: 1419604-27-5
phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

Guidance literature:: With pyridine; In acetone; at 0 - 23 ℃; for 1h;

Reference yield:

: 55338-73-3
5-amino-2-cyanopyridine

: 1419604-27-5
phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 - 23 °C

2: diisobutylaluminium hydride / tetrahydrofuran; toluene / 3 h / -78 °C

3: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 3 h / 0 - 23 °C

4: sulfuric acid / 3 h / 50 °C

5: pyridine / acetone / 1 h / 0 - 23 °C

With pyridine; sulfuric acid; sodium tris(acetoxy)borohydride; sodium hydride; diisobutylaluminium hydride; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 1419604-19-5
5-(dibenzylamino)picolinonitrile

: 1419604-27-5
phenyl 6-((2-methoxyethylamino)methyl)pyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 3 h / -78 °C

2: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 3 h / 0 - 23 °C

3: sulfuric acid / 3 h / 50 °C

4: pyridine / acetone / 1 h / 0 - 23 °C

With pyridine; sulfuric acid; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; acetic acid; In tetrahydrofuran; acetone; toluene;