4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide

Base Information

Chemical Name:4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide
CAS No.:1363789-11-0
Molecular Formula:C₂F₆NO₄S₂*C₆H₄BrN₂
Molecular Weight:464.164
Hs Code.:

Synonyms:4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide

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Technology Process of 4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide

There total 2 articles about 4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: (x)BF₄*C₆H₄BrN₂⁽¹⁺⁾

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1363789-11-0
4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide

Guidance literature:: In acetonitrile; for 0.5h;
DOI:10.1016/j.jfluchem.2011.10.016

Reference yield:

: 82113-65-3
bis(trifluoromethanesulfonyl)amide

: 106-40-1
4-bromo-aniline

: 1363789-11-0
4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide

Guidance literature:: 4-bromo-aniline; With hydrogenchloride; In water; at 0 ℃; for 0.166667h;

With sodium nitrite; In water; at 0 ℃; for 0.5h;

bis(trifluoromethanesulfonyl)amide; at 0 ℃; for 0.166667h;

Reference yield: 36.0%

: 1363789-11-0
4-bromobenzenediazonium bis((trifluoromethyl)sulfonyl)amide

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 89901-03-1
methyl 4’-bromo-[1,1’-diphenyl]-4-carboxylate

Guidance literature:: With chloro[tris(para-trifluoromethylphenyl)phosphine]gold (I); cesium fluoride; In methanol; at 20 ℃; for 15h; Reagent/catalyst; Irradiation; Inert atmosphere;