S-(4-methoxyphenyl) benzenesulfinothioate

Base Information

Chemical Name:S-(4-methoxyphenyl) benzenesulfinothioate
CAS No.:26974-26-5
Molecular Formula:C₁₃H₁₂O₂S₂
Molecular Weight:264.369
Hs Code.:

Synonyms:Benzenesulfinicacid, thio-, S-(p-methoxyphenyl) ester (7CI,8CI); Benzenesulfinothioic acid,S-(4-methoxyphenyl) ester (9CI); Benzenethiol, p-methoxy-, benzenesulfinate(8CI); NSC 243182

Suppliers and Price of S-(4-methoxyphenyl) benzenesulfinothioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of S-(4-methoxyphenyl) benzenesulfinothioate

Chemical Property:

Vapor Pressure:9.19E-08mmHg at 25°C
Boiling Point:447°Cat760mmHg
Flash Point:224.1°C
Density:1.34g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of S-(4-methoxyphenyl) benzenesulfinothioate

There total 4 articles about S-(4-methoxyphenyl) benzenesulfinothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95914-29-7
1-(4-methoxyphenyl)-2-phenyldisulfane

: 26974-26-5,133670-28-7,133751-12-9
S-(4-methoxyphenyl) benzenethiosulfinate

: 26974-29-8,133670-29-8,133751-13-0
S-phenyl 4-methoxybenzenesulfinothioate

Guidance literature:: With 3H-2,1-benzoxaselenole Se-oxide; dihydrogen peroxide; In methanol; dichloromethane; at 20 ℃; for 3h; Overall yield = 43 %;
DOI:10.3390/molecules200610748

Reference yield:

: 882-33-7
diphenyldisulfane

: 26974-26-5,133670-28-7,133751-12-9
S-(4-methoxyphenyl) benzenethiosulfinate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl chloride / acetic anhydride / 0.33 h / 0 °C

2: diethyl ether; pyridine / 0.33 h / 20 °C

With sulfuryl dichloride; In pyridine; diethyl ether; acetic anhydride; 1: Oxidation / 2: Condensation;
DOI:10.1021/ol006715o