4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate

Base Information

Chemical Name:4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate
CAS No.:1448297-12-8
Molecular Formula:C₂₁H₂₀F₃NO₇S₂
Molecular Weight:519.52
Hs Code.:

Synonyms:4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate

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Chemical Property of 4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate

Chemical Property:

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Technology Process of 4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate

There total 3 articles about 4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448297-19-5
4-[(2-butyl-5-amino-1-benzofuran-3-yl)carbonyl]phenyltrifluoromethanesulfonate

: 124-63-0
methanesulfonyl chloride

: 1448297-12-8
4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 30 - 35 ℃; for 4.5h;

Reference yield:

: 1448297-17-3
4-[(2-butyl-5-nitro-1-benzofuran-3-yl)carbonyl]phenyltrifluoromethanesulfonate

: 1448297-12-8
4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 6.5 h / 75 °C / 7500.75 Torr

2: pyridine / dichloromethane / 4.5 h / 30 - 35 °C

With pyridine; palladium 10% on activated carbon; hydrogen; In ethanol; dichloromethane;

Reference yield:

: 141645-16-1
2-n-butyl-3-(4-hydroxybenzoyl)-5-nitrobenzofuran

: 1448297-12-8
4-({2-butyl-5-[(methylsulfonyl)amino]-1-benzofuran-3-yl}carbonyl)phenyltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 5.5 h / 20 °C / Reflux

2: palladium 10% on activated carbon; hydrogen / ethanol / 6.5 h / 75 °C / 7500.75 Torr

3: pyridine / dichloromethane / 4.5 h / 30 - 35 °C

With pyridine; palladium 10% on activated carbon; hydrogen; triethylamine; In ethanol; dichloromethane;