2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide

Base Information

• Chemical Name: 2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide
• CAS No.: 111508-36-2
• Molecular Formula: C₁₉H₂₂N₂O₄
• Molecular Weight: 342.395

Synonyms:2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide

Chemical Property of 2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide

Chemical Property:

Purity/Quality:

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Technology Process of 2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide

There total 2 articles about 2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

ethanol (64-17-5) + ethyl 3-oxo-3-(phenylamino)propionate (53341-66-5) + Nitrosobenzene (586-96-9) → 2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide (111508-36-2)

Guidance literature:

With sodium carbonate; In water; for 4h;

DOI:10.1039/P19870000877

Reference yield:

aniline (62-53-3) → 2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide (111508-36-2)

Guidance literature:

Multi-step reaction with 2 steps

2: 59 percent / Na₂CO₃ / H₂O / 4 h

With sodium carbonate; In water;

DOI:10.1039/P19870000877

Reference yield: 100.0%

2-ethoxy-2-phenylaminomalonic acid monoethyl ester N-phenylcarboxamide (111508-36-2) → 2-phenyliminomalonic acid monoethyl ester N-phenylcarboxamide (93847-24-6)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 2h; Heating;

DOI:10.1039/P19870000877

upstream raw materials:

ethanol

ethyl 3-oxo-3-(phenylamino)propionate

Nitrosobenzene

aniline

Downstream raw materials:

2-phenyliminomalonic acid monoethyl ester N-phenylcarboxamide

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