3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

Base Information

Chemical Name:3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid
CAS No.:1422953-13-6
Molecular Formula:C₂₆H₃₈O₆
Molecular Weight:446.584
Hs Code.:

Synonyms:3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

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Chemical Property of 3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

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Technology Process of 3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

There total 4 articles about 3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422953-12-5
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzaldehyde

: 1422953-13-6
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 25 ℃; for 8h;
DOI:10.1055/s-0032-1317544

Reference yield:

: 1422953-11-4
{3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]phenyl}methanol

: 1422953-13-6
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane / 3 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

2: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 8 h / 25 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; pyridinium chlorochromate; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1055/s-0032-1317544

Reference yield:

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 1422953-13-6
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butyl lithium; N,N,N,N,-tetramethylethylenediamine; copper(I) bromide dimethylsulfide complex / pentane; tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

1.2: 2 h / -20 °C / Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 3 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

3.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 8 h / 25 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; copper(I) bromide dimethylsulfide complex; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; pentane;
DOI:10.1055/s-0032-1317544