N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide

Base Information

Chemical Name:N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide
CAS No.:1422953-14-7
Molecular Formula:C₃₀H₄₇NO₅
Molecular Weight:501.707
Hs Code.:

Synonyms:N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide

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Chemical Property of N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide

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Technology Process of N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide

There total 5 articles about N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1422953-13-6
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzoic acid

: 660-68-4
diethyl amine hydrochloride

: 1422953-14-7
N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 25 ℃; for 24h; Inert atmosphere;
DOI:10.1055/s-0032-1317544

Reference yield:

: 76280-60-9
[3,5-bis(methoxymethoxy)phenyl]methanol

: 1422953-14-7
N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butyl lithium; N,N,N,N,-tetramethylethylenediamine; copper(I) bromide dimethylsulfide complex / pentane; tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

1.2: 2 h / -20 °C / Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 3 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

3.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 8 h / 25 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 25 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; copper(I) bromide dimethylsulfide complex; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; pentane;
DOI:10.1055/s-0032-1317544

Reference yield:

: 1422953-11-4
{3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]phenyl}methanol

: 1422953-14-7
N,N-diethyl-3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate / dichloromethane / 3 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

2: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 8 h / 25 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 25 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1055/s-0032-1317544