methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate

Base Information

Chemical Name:methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate
CAS No.:941608-29-3
Molecular Formula:C₂₁H₂₄BrFN₂O₇S
Molecular Weight:547.399
Hs Code.:

Synonyms:methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate

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Chemical Property of methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate

Chemical Property:

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Technology Process of methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate

There total 11 articles about methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)amino)acetate

: 147000-89-3
N-tert-butyloxycarbonylsulfamoyl chloride

: 941608-29-3
methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)amino)acetate

: 75-65-0
tert-butyl alcohol

: 941608-29-3
methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate

Guidance literature:: isocyanate de chlorosulfonyle; tert-butyl alcohol; In dichloromethane; at 0 - 10 ℃; for 0.5h;

methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)amino)acetate; With triethylamine; In dichloromethane; at 10 - 20 ℃; for 0.5h;

Reference yield:

: 941608-28-2
2-(benzyloxy)-4-bromo-6-fluoroaniline

: 941608-29-3
methyl 2-((2-(benzyloxy)-4-bromo-6-fluorophenyl)(N-(tert-butoxycarbonyl)sulfamoyl)amino)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

2: triethylamine / dichloromethane / 3 h / 20 °C

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;