ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate

Base Information

Chemical Name:ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate
CAS No.:1357621-05-6
Molecular Formula:C₁₉H₂₀Cl₃N₃O₄
Molecular Weight:460.745
Hs Code.:

Synonyms:ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate

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Chemical Property of ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate

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Technology Process of ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate

There total 4 articles about ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl 2-(3-(5-amino-3-cyclopropyl-1H-pyrazol-1-yl)phenyl)acetate

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1357621-05-6
ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate

Guidance literature:: With sodium hydroxide; In water; ethyl acetate; at 0 - 20 ℃; for 2.5h;
DOI:10.1016/j.ejmech.2011.11.019

Reference yield:

: 1357621-00-1
2-(3-(carboxymethyl)phenyl)hydrazinium chloride

: 1357621-05-6
ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: Reflux

2: sodium hydroxide / water; ethyl acetate / 2.5 h / 0 - 20 °C

With sodium hydroxide; In water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.11.019

Reference yield:

: 14338-36-4
3-amino phenylacetic acid

: 1357621-05-6
ethyl [3-(3-cyclopropyl-5-{[(2,2,2-trichloroethoxy)carbonyl]amino}-1H-pyrazol-1-yl)phenyl]acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

1.2: 2 h / 0 - 20 °C

2.1: Reflux

3.1: sodium hydroxide / water; ethyl acetate / 2.5 h / 0 - 20 °C

With hydrogenchloride; sodium hydroxide; sodium nitrite; In water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.11.019