trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate)

Base Information

Chemical Name:trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate)
CAS No.:1610688-91-9
Molecular Formula:C₃₉H₂₁Cl₃F₃N₃O₉
Molecular Weight:838.965
Hs Code.:

Synonyms:trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate)

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Chemical Property of trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate)

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Technology Process of trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate)

There total 2 articles about trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1391943-72-8
(E)-methyl 3-(2-chloro-6-fluorophenyl)-5-(2-(dimethylamino)vinyl)isoxazole-4-carboxylate

: 1610688-91-9
trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate)

Guidance literature:: With acetyl chloride; In 1,4-dioxane; at 50 ℃; for 216h;
DOI:10.1016/j.tet.2014.04.015

Reference yield:

: 4415-09-2
methyl 3-(2-chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylate

: 1610688-91-9
trimethyl 5,5',5-(benzene-1,3,5-triyl)tris(3-(2-chloro-6-fluorophenyl)isoxazole-4-carboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-1H-imidazole / 6 h / 80 °C

2: acetyl chloride / 1,4-dioxane / 216 h / 50 °C

With 1-methyl-1H-imidazole; acetyl chloride; In 1,4-dioxane;
DOI:10.1016/j.tet.2014.04.015