Technology Process of C26H22N2O3S
There total 3 articles about C26H22N2O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/jm3013097
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.25 h / Cooling with ice; Inert atmosphere
1.2: 12 h / 60 °C / Inert atmosphere
2.1: potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / N,N-dimethyl-formamide / 12 h / 110 °C / Inert atmosphere
With
potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm3013097
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.25 h / Cooling with ice; Inert atmosphere
1.2: 12 h / 60 °C / Inert atmosphere
2.1: potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / N,N-dimethyl-formamide / 12 h / 110 °C / Inert atmosphere
With
potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm3013097
