2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

Base Information

Chemical Name:2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide
CAS No.:577795-02-9
Molecular Formula:C₂₄H₃₅N₅O₃
Molecular Weight:441.574
Hs Code.:

Synonyms:2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

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Chemical Property of 2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

Chemical Property:

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Technology Process of 2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

There total 3 articles about 2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-36-7
N,N-diethylethylenediamine

: 433728-66-6
2-(6-chloro-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

: 577795-02-9
2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 65 ℃;
DOI:10.1021/jm030109s

Reference yield:

: 16013-85-7,136901-10-5
2,6-dicholoro-3-nitropyridine

: 577795-02-9
2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / K₂CO₃; [Pd(PPh₃)4] / toluene; ethanol; H₂O / 80 °C

2: 92 percent / ethyldiisopropylamine / tetrahydrofuran / 65 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; water; toluene; 1: Suzuki coupling;
DOI:10.1021/jm030109s

Reference yield:

: 103681-98-7
2-diisopropylaminocarbonylphenylboronic acid

: 577795-02-9
2-(6-{[2-(diethylamino)ethyl]amino}-3-nitropyridin-2-yl)-N,N-diisopropylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / K₂CO₃; [Pd(PPh₃)4] / toluene; ethanol; H₂O / 80 °C

2: 92 percent / ethyldiisopropylamine / tetrahydrofuran / 65 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; water; toluene; 1: Suzuki coupling;
DOI:10.1021/jm030109s