C₂₁H₂₂N₆O₄

Base Information

Chemical Name:C₂₁H₂₂N₆O₄
CAS No.:1311407-03-0
Molecular Formula:C₂₁H₂₂N₆O₄
Molecular Weight:422.443
Hs Code.:

C<sub>21</sub>H<sub>22</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₂₁H₂₂N₆O₄

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Chemical Property of C₂₁H₂₂N₆O₄

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Technology Process of C₂₁H₂₂N₆O₄

There total 19 articles about C₂₁H₂₂N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1311407-01-8
C₂₉H₂₉N₇O₆

: 1311407-03-0
C₂₁H₂₂N₆O₄

Guidance literature:: With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; at 0 - 20 ℃; for 24h;
DOI:10.1021/jo2004617

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 1311407-03-0
C₂₁H₂₂N₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / toluene / Reflux

2: lithium hexamethyldisilazane / tetrahydrofuran

3: di-isopropyl azodicarboxylate; acetic acid; triphenylphosphine / tetrahydrofuran

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

5: pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 24 h / 0 - 20 °C

With pyridine; di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; 3: Mitsunobu reaction / 4: Mitsunobu reaction;
DOI:10.1021/jo2004617

Reference yield:

: 100-52-7
benzaldehyde

: 1311407-03-0
C₂₁H₂₂N₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / toluene / 60 h / Reflux; Dean-Stark

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

4: pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 24 h / 0 - 20 °C

With pyridine; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; toluene; 3: Mitsunobu reaction;
DOI:10.1021/jo2004617