5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine

Base Information

• Chemical Name: 5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine
• CAS No.: 1020085-39-5
• Molecular Formula: C₄₇H₈₄N₄O₆Si₄
• Molecular Weight: 913.549

Synonyms:5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine

Chemical Property of 5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine

Chemical Property:

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Technology Process of 5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine

There total 1 articles about 5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

2,4-bis(benzyloxy)-5-nitro-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine (1020085-38-4) → 5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine (1020085-39-5)

Guidance literature:

With sodium dithionite; In methanol; water; at 90 ℃; for 5.5h;

DOI:10.1021/jo702631a

Reference yield: 92.0%

5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine (1020085-39-5) + chloroacetyl chloride (79-04-9) → N-[2,4-bis(benzyloxy)-6-{[(2S,3S,4R)-2,3,4,5-tetrakis[(tert-butyldimethylsilyl)oxy]pentyl]amino}pyrimidin-5-yl]-2-chloroacetamide (1389329-05-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;

DOI:10.1021/jo3010364

Reference yield: 87.0%

5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine (1020085-39-5) + 2-chloropropionyl chloride (7623-09-8) → N-[2,4-bis(benzyloxy)-6-{[(2S,3S,4R)-2,3,4,5-tetrakis[(tert-butyldimethylsilyl)oxy]pentyl]amino}pyrimidin-5-yl]-2-chloropropanamide (1389329-02-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;

DOI:10.1021/jo3010364

upstream raw materials:

2,4-bis(benzyloxy)-5-nitro-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine

Downstream raw materials:

N-(2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-O-(tert-butyldimethylsilyl)ribitylamino]pyrimidin-5-yl)propionamide

N-{2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidin-5-yl}oxalamic acid ethyl ester

N-(2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-O-(tert-butyldimethylsilyl)ribitylamino]pyrimidin-5-yl)isobutyramide

N-[2,4-bis(benzyloxy)-6-{[(2S,3S,4R)-2,3,4,5-tetrakis[(tert-butyldimethylsilyl)oxy]pentyl]amino}pyrimidin-5-yl]-2-chloropropanamide

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