[(o-EtC₆H₄)CH₂]2SnPh₂

Base Information

Chemical Name:[(o-EtC₆H₄)CH₂]2SnPh₂
CAS No.:1206710-35-1
Molecular Formula:C₃₀H₃₂Sn
Molecular Weight:511.294
Hs Code.:

[(o-EtC<sub>6</sub>H<sub>4</sub>)CH<sub>2</sub>]2SnPh<sub>2</sub>

Synonyms:[(o-EtC₆H₄)CH₂]2SnPh₂

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Chemical Property of [(o-EtC₆H₄)CH₂]2SnPh₂

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Technology Process of [(o-EtC₆H₄)CH₂]2SnPh₂

There total 1 articles about [(o-EtC₆H₄)CH₂]2SnPh₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1467-06-7
2-ethylbenzyl chloride

: 1135-99-5
diphenyltin(IV) dichloride

: 1206710-35-1
[(o-EtC₆H₄)CH₂]2SnPh₂

Guidance literature:: With Mg; In tetrahydrofuran; (N2) Ph2SnCl2 was added to mixt. benzyl chloride and Mg in THF at 0°C, react. mixt. was kept at 0°C and allowed to stir overnight; solvent was removed in vacuo, residue was extd. with hexane and filtered, recrystn. from hexane at -20°C; elem. anal.;
DOI:10.1021/ic901800c

Reference yield: 90.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 1206710-35-1
[(o-EtC₆H₄)CH₂]2SnPh₂

: 1206710-36-2
[(o-EtC₆H₄)CH₂]2SnPhCl

Guidance literature:: In diethyl ether; benzene; (N2) soln. HCl in Et2O was added dropwise to soln. Sn complex in benzene, stirred for 30 min; solvent was removed in vacuo; elem. anal.;
DOI:10.1021/ic901800c