(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester

Base Information

• Chemical Name: (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester
• CAS No.: 1265883-87-1
• Molecular Formula: C₂₉H₄₀O₅Si
• Molecular Weight: 496.719

Synonyms:(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester

Chemical Property of (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester

There total 10 articles about (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester (1265883-86-0) + N,N-dimethylformamide di-tert-butyl acetal (36805-97-7) → (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester (1265883-87-1)

Guidance literature:

In toluene; at 110 ℃; for 1.5h; Reflux;

Reference yield: 82.0%

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester (1265883-86-0) + N,N-dimethylformamide di-tert-butyl acetal (36805-97-7) → (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester (1265883-87-1) + (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester (1265883-88-2)

Guidance literature:

In toluene;

Reference yield:

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester (1265883-85-9) → (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester (1265883-86-0) + (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester (1265883-87-1)

Guidance literature:

With H₂; nitrogen; palladium-carbon; In ethanol;

upstream raw materials:

(1R,6S)-6-methoxycarbonyl-3-cyclohexene-1-carboxylic acid

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester

N,N-dimethylformamide di-tert-butyl acetal

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

Downstream raw materials:

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester

(1R,2R,4R)-5-(tert-butyldiphenylsilanyloxy)-2-(hex-5-enyl-methylcarbamoyl)cyclohexanecarboxylic acid tert-butyl ester

(1R,2R,4R)-5-(tert-butyldiphenylsilanyloxy)-2-(hex-5-enyl-methylcarbamoyl)cyclohexanecarboxylic acid

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