(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester

Base Information

• Chemical Name: (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester
• CAS No.: 1265883-86-0
• Molecular Formula: C₂₅H₃₂O₅Si
• Molecular Weight: 440.612

Synonyms:(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester

Chemical Property of (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester

There total 9 articles about (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester (1265883-85-9) → (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester (1265883-86-0)

Guidance literature:

With hydrogen; palladium on carbon; In ethanol; for 16h; Inert atmosphere;

Reference yield: 65.0%

1H-imidazole (288-32-4) + (1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester (1265882-90-3) → (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester (1265883-86-0) + (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester (1265883-85-9)

Guidance literature:

In N,N-dimethyl-formamide;

Reference yield:

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester (1265883-85-9) → (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 1-methyl ester (1265883-86-0) + (1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester (1265883-87-1)

Guidance literature:

With H₂; nitrogen; palladium-carbon; In ethanol;

upstream raw materials:

(1R,6S)-6-methoxycarbonyl-3-cyclohexene-1-carboxylic acid

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

(1R,2R)-cyclohex-4-ene 1,2-dicarboxylic acid monomethyl ester

(1R,2R,4R,5S)-4-iodo-7-oxo-6-oxabicyclo[3.2.1]-octane-2-carboxylic acid methyl ester

Downstream raw materials:

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester 1-methyl ester

(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-tert-butyl ester

(1R,2R,4R)-5-(tert-butyldiphenylsilanyloxy)-2-(hex-5-enyl-methylcarbamoyl)cyclohexanecarboxylic acid tert-butyl ester

(1R,2R,4R)-5-(tert-butyldiphenylsilanyloxy)-2-(hex-5-enyl-methylcarbamoyl)cyclohexanecarboxylic acid

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