methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside

Base Information

Chemical Name:methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside
CAS No.:91925-96-1
Molecular Formula:C₁₇H₂₃NO₆
Molecular Weight:337.373
Hs Code.:

Synonyms:methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside

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Technology Process of methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside

There total 7 articles about methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 91897-37-9
methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-α-D-mannopyranoside

: 74-88-4
methyl iodide

: 91925-96-1
methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 1.5h; Ambient temperature;

Reference yield:

: 98237-78-6
((2R,3S,4S,5S,6S)-3,5-Dihydroxy-2-hydroxymethyl-6-methoxy-tetrahydro-pyran-4-yl)-carbamic acid benzyl ester

: 91925-96-1
methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 36 h / Ambient temperature

2: H₂ / 10percent Pd/C / ethanol / 18 h / 3192 Torr

3: CH₃COONa / ethanol / 8 h / Heating

4: NaHCO₃ / ethanol; H₂O / 2 h / ice-cooling

5: 67 percent / 1.) NaH / dimethylformamide / 1.5 h / Ambient temperature

With hydrogen; sodium acetate; sodium hydride; sodium hydrogencarbonate; palladium on activated charcoal; In pyridine; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 91897-27-7
methyl 3-benzyloxycarbonylamino-3-deoxy-6-O-tosyl-α-D-mannopyranoside

: 91925-96-1
methyl 3,6-benzyloxycarbonylimino-3,6-dideoxy-2,4-di-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / ethanol / 18 h / 3192 Torr

2: CH₃COONa / ethanol / 8 h / Heating

3: NaHCO₃ / ethanol; H₂O / 2 h / ice-cooling

4: 67 percent / 1.) NaH / dimethylformamide / 1.5 h / Ambient temperature

With hydrogen; sodium acetate; sodium hydride; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; water; N,N-dimethyl-formamide;