p-flurobenzoylpivaloylmethanate

Base Information

Chemical Name:p-flurobenzoylpivaloylmethanate
CAS No.:68490-55-1
Molecular Formula:C₁₃H₁₅FO₂
Molecular Weight:222.259
Hs Code.:

Synonyms:p-flurobenzoylpivaloylmethanate

Suppliers and Price of p-flurobenzoylpivaloylmethanate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of p-flurobenzoylpivaloylmethanate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of p-flurobenzoylpivaloylmethanate

There total 1 articles about p-flurobenzoylpivaloylmethanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-97-8
3,3-dimethyl-butan-2-one

: 403-43-0
4-fluorobenzoyl chloride

: 68490-55-1
p-flurobenzoylpivaloylmethanate

Guidance literature:: 3,3-dimethyl-butan-2-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;

4-fluorobenzoyl chloride; In tetrahydrofuran; at 0 ℃; for 5h; Inert atmosphere;
DOI:10.1055/a-1409-1906

Reference yield:

: 68490-55-1
p-flurobenzoylpivaloylmethanate

: 2-diazo-1-(4-fluorophenyl)-4,4-dimethylpentane-1,3-dione

Guidance literature:: With 4-acetamidobenzenesulfonyl azide; triethylamine; In acetonitrile; at 0 - 20 ℃; for 12h;
DOI:10.1055/a-1409-1906

Reference yield:

: 10124-27-3
aluminum chloride hexahydrate

: 68490-55-1
p-flurobenzoylpivaloylmethanate

: 154936-49-9
tris(p-flurobenzoylpivaloylmethanato)aluminium(III)

Guidance literature:: With sodium acetate; In methanol; water; addn. of p-flurobenzoylpivaloylmethanate in methanol to a stirred soln.of AlCl3*6H2O and sodium acetate in H2O; stirring for 1 h at ambient temperature; filtration;; washing with water/methanol (1:1); recrystallization from ethanol with benzene for 3 times; drying in vac. at 100°C; elem. anal.;;
DOI:10.1016/0040-6031(94)80067-7