5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine

Base Information

Chemical Name:5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine
CAS No.:516509-89-0
Molecular Formula:C₄₂H₄₈N₈O₈P₂
Molecular Weight:854.839
Hs Code.:

Synonyms:5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine

Chemical Property:

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Technology Process of 5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine

There total 5 articles about 5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 65370-94-7
1-(5-hydroxypentyl)-2',3'-O-isopropylideneinosine

: 5625-99-0
N,N'-diphenylphosphorodiamidic chloride

: 516509-89-0
5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1002/1099-0690(200212)2002:24<4234::AID-EJOC4234>3.0.CO;2-8

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 516509-89-0
5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / dimethylformamide / 6 h / 80 °C

2: 8 percent / pyridine / 12 h / 20 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200212)2002:24<4234::AID-EJOC4234>3.0.CO;2-8

Reference yield:

: 15888-39-8
((3aR,4R,6R,6aR)-2,2-dimethyl-6-(6-oxo-1,6-dihydro-9H-purin-9-yl)tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl acetate

: 516509-89-0
5'-O-(dianilinophosphoryl)-1-[5-O-(dianilinophosphoryl)pentyl]-2',3'-O-isopropylideneinosine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃ / dimethylformamide / 2.5 h / 80 °C

2: 85 percent / dimethylformamide / 6 h / 80 °C

3: 8 percent / pyridine / 12 h / 20 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200212)2002:24<4234::AID-EJOC4234>3.0.CO;2-8