6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Base Information

Chemical Name:6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane
CAS No.:615269-59-5
Molecular Formula:C₅₃H₇₁N₃O₆S₃
Molecular Weight:942.361
Hs Code.:

Synonyms:6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

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Chemical Property of 6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

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Technology Process of 6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

There total 4 articles about 6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 615269-56-2
1,11-bis(tert-butyloxycarbonyl)-6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

: 615269-59-5
6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 7h;
DOI:10.1002/ejoc.200300171

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 615269-59-5
6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / potassium carbonate / acetonitrile / 14 h / Heating

2: 95 percent / trifluoroacetic acid / CH₂Cl₂ / 7 h / 20 °C

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200300171

Reference yield:

: 91-13-4
α,α'-dibromo-o-xylene

: 615269-59-5
6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / potassium carbonate / acetonitrile / 14 h / Heating

2: 82 percent / potassium carbonate / acetonitrile / 14 h / Heating

3: 95 percent / trifluoroacetic acid / CH₂Cl₂ / 7 h / 20 °C

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200300171