11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

Base Information

Chemical Name:11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane
CAS No.:615269-62-0
Molecular Formula:C₆₁H₇₇N₃O₆S₃
Molecular Weight:1044.5
Hs Code.:

Synonyms:11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

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Chemical Property of 11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

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Technology Process of 11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

There total 4 articles about 11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 91-13-4
α,α'-dibromo-o-xylene

: 615269-59-5
6-[(4-methylphenyl)sulfonyl]-1,11-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

: 615269-62-0
11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

Guidance literature:: With potassium carbonate; In acetonitrile; Heating;
DOI:10.1002/ejoc.200300171

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 615269-62-0
11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / potassium carbonate / acetonitrile / 14 h / Heating

2: 95 percent / trifluoroacetic acid / CH₂Cl₂ / 7 h / 20 °C

3: 97 percent / potassium carbonate / acetonitrile / Heating

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200300171

Reference yield:

: 335004-12-1
N-(tert-butyloxycarbonyl)(2,4,6-triisopropylphenyl)sulfonamide

: 615269-62-0
11-[(4-methylphenyl)sulfonyl]-1,6-bis[(2,4,6-triisopropylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / potassium carbonate / acetonitrile / 14 h / Heating

2: 82 percent / potassium carbonate / acetonitrile / 14 h / Heating

3: 95 percent / trifluoroacetic acid / CH₂Cl₂ / 7 h / 20 °C

4: 97 percent / potassium carbonate / acetonitrile / Heating

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200300171