1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one

Base Information

Chemical Name:1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one
CAS No.:1026056-70-1
Molecular Formula:C₂₀H₂₄O₉
Molecular Weight:408.405
Hs Code.:

Synonyms:1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one

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Chemical Property of 1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one

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Technology Process of 1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one

There total 4 articles about 1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026163-30-3
2-(3-Benzyloxy-4-methoxy-phenyl)-1-(3,6-bis-benzyloxy-2,4-dimethoxy-phenyl)-3,3-dimethoxy-propan-1-one

: 1026056-70-1
1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; Ambient temperature;
DOI:10.1248/cpb.44.486

Reference yield:

: 6962-57-8
3,6-dihydroxy-2,4-dimethoxyacetophenone

: 1026056-70-1
1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / potassium carbonate / dimethylformamide / 0.17 h / 160 °C

2: 83 percent / KOH / ethanol / 50 °C

3: 1.)Tl(NO₃)3*3H₂O, 2.)Na₂SO₃, 5percent HCl / 1.) CHCl₃, 30 deg C, 24 h 2.) 0 deg C

4: H₂ / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature

With hydrogenchloride; potassium hydroxide; hydrogen; potassium carbonate; thallium(III) nitrate; sodium sulfite; palladium on activated charcoal; In methanol; ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.44.486

Reference yield:

: 175988-38-2
1-(3,6-Bis-benzyloxy-2,4-dimethoxy-phenyl)-ethanone

: 1026056-70-1
1-(3,6-Dihydroxy-2,4-dimethoxy-phenyl)-2-(3-hydroxy-4-methoxy-phenyl)-3,3-dimethoxy-propan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / KOH / ethanol / 50 °C

2: 1.)Tl(NO₃)3*3H₂O, 2.)Na₂SO₃, 5percent HCl / 1.) CHCl₃, 30 deg C, 24 h 2.) 0 deg C

3: H₂ / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature

With hydrogenchloride; potassium hydroxide; hydrogen; thallium(III) nitrate; sodium sulfite; palladium on activated charcoal; In methanol; ethanol; ethyl acetate;
DOI:10.1248/cpb.44.486