{4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

Base Information

Chemical Name:{4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester
CAS No.:476360-67-5
Molecular Formula:C₂₃H₂₀N₆O₅
Molecular Weight:460.449
Hs Code.:

{4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3<i>H</i>-1,3,4,5,7a-pentaaza-<i>s</i>-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

Synonyms:{4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

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Chemical Property of {4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

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Technology Process of {4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

There total 4 articles about {4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 59277-89-3
acycloguanosine

: 476360-60-8
4-[(phenoxycarbonyl)amino]phenacyl bromide

: 476360-67-5
{4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

Guidance literature:: acycloguanosine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

4-[(phenoxycarbonyl)amino]phenacyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Further stages.;
DOI:10.1021/jm020827z

Reference yield:

: 99-92-3
p-aminobenzophenone

: 476360-67-5
{4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 5 h / 20 °C

2.1: Br₂; AlCl₃ / tetrahydrofuran / 2 h / 0 - 20 °C

3.1: NaH / dimethylformamide / 1 h / 20 °C

3.2: 18 percent / dimethylformamide / 4 h / 20 °C

With pyridine; aluminium trichloride; bromine; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm020827z

Reference yield:

: 1885-14-9
phenyl chloroformate

: 476360-67-5
{4-[3-(2-hydroxy-ethoxymethyl)-8-oxo-5,8-dihydro-3H-1,3,4,5,7a-pentaaza-s-indacen-6-yl]-phenyl}-carbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 5 h / 20 °C

2.1: Br₂; AlCl₃ / tetrahydrofuran / 2 h / 0 - 20 °C

3.1: NaH / dimethylformamide / 1 h / 20 °C

3.2: 18 percent / dimethylformamide / 4 h / 20 °C

With pyridine; aluminium trichloride; bromine; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm020827z