O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate

Base Information

Chemical Name:O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate
CAS No.:1346434-19-2
Molecular Formula:C₂₈H₃₀N₂O₄
Molecular Weight:458.557
Hs Code.:

Synonyms:O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate

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Chemical Property of O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate

Chemical Property:

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Technology Process of O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate

There total 8 articles about O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) chloroformate

: 62-53-3
aniline

: 1346434-19-2
O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate

Guidance literature:: With water; sodium hydrogencarbonate; In acetone; for 0.5h;

Reference yield:

: 1346434-17-0
2-((N-tBOC-N-methylamino)methyl)fluorene

: 1346434-19-2
O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

1.2: -78 - 20 °C

2.1: sodium tetrahydroborate / methanol

3.1: pyridine / tetrahydrofuran / 1 h / 20 °C / Cooling with ice

4.1: sodium hydrogencarbonate; water / acetone / 0.5 h

With pyridine; sodium tetrahydroborate; water; sodium hydrogencarbonate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; acetone;

Reference yield:

: 1346434-18-1
9-(2-(N-tBOC-N-methylamino)methyl)fluorenylmethanol

: 1346434-19-2
O-(9-(2-((N-tBOC-N-methylamino)methyl)fluorenylmethyl)) N-phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 1 h / 20 °C / Cooling with ice

2: sodium hydrogencarbonate; water / acetone / 0.5 h

With pyridine; water; sodium hydrogencarbonate; In tetrahydrofuran; acetone;