4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester

Base Information

Chemical Name:4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester
CAS No.:120533-79-1
Molecular Formula:C₁₉H₂₁F₂NO₃S₂
Molecular Weight:413.509
Hs Code.:

Synonyms:4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester

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Chemical Property of 4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester

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Technology Process of 4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester

There total 3 articles about 4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 120533-90-6
4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

: 120533-79-1
4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester

Guidance literature:: With Lawessons reagent; In xylene; for 6h; Heating;
DOI:10.1007/BF00474047

Reference yield:

: 120533-64-4
4-(2-Difluoromethoxy-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

: 120533-79-1
4-(2-Difluoromethoxy-phenyl)-1-methyl-1,4-dihydro-pyridine-3,5-dicarbothioic acid di-O-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Lawesson's reagent / xylene / 25 h / Heating

2: 1. KOH / 1. 1,2-dimethoxyethane, reflux, 5 min; 2. reflux, 5 min

With Lawessons reagent; potassium hydroxide; In xylene;
DOI:10.1007/BF00474047