Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid
CAS No.:112622-79-4
Molecular Formula:C₇₅H₈₄N₂O₁₉
Molecular Weight:1317.49
Hs Code.:

Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Synonyms:Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Suppliers and Price of Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

There total 9 articles about Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 112622-79-4
Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

2: 92 percent / pyridine

3: 92 percent / NaBH₃CN, HCl, molecular sieve / tetrahydrofuran; diethyl ether / 0 °C

4: 92 percent / CF₃SO₃Ag, collidine, molecular sieve / CH₂Cl₂ / 6 h / -50 - -30 °C

5: H₂S / pyridine; H₂O; triethylamine / 24 h

6: pyridine / 5 h

With pyridine; 2,3,5-trimethyl-pyridine; hydrogenchloride; molecular sieve; hydrogen sulfide; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; diethyl ether; dichloromethane; water; triethylamine; N,N-dimethyl-formamide;

Reference yield:

: 110236-58-3
Methyl-3,6-di-O-benzyl-4-O-(3-O-benzyl-α-L-idopyranosyl)-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

: 112622-79-4
Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

2: 92 percent / pyridine

3: 92 percent / NaBH₃CN, HCl, molecular sieve / tetrahydrofuran; diethyl ether / 0 °C

4: 92 percent / CF₃SO₃Ag, collidine, molecular sieve / CH₂Cl₂ / 6 h / -50 - -30 °C

5: H₂S / pyridine; H₂O; triethylamine / 24 h

6: pyridine / 5 h

With pyridine; 2,3,5-trimethyl-pyridine; hydrogenchloride; molecular sieve; hydrogen sulfide; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; diethyl ether; dichloromethane; water; triethylamine; N,N-dimethyl-formamide;

Reference yield:

: 110236-57-2
Acetic acid (2S,3R,4S,5R,6S)-5-acetoxy-6-acetoxymethyl-4-benzyloxy-2-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-tetrahydro-pyran-3-yl ester

: 112622-79-4
Methyl-O-<6-O-acetyl-2-(acetylamino)-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl>-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 7 steps

1: 92 percent / 1 N CH₃ONa / methanol / 12 h

2: 89 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

3: 92 percent / pyridine

4: 92 percent / NaBH₃CN, HCl, molecular sieve / tetrahydrofuran; diethyl ether / 0 °C

5: 92 percent / CF₃SO₃Ag, collidine, molecular sieve / CH₂Cl₂ / 6 h / -50 - -30 °C

6: H₂S / pyridine; H₂O; triethylamine / 24 h

7: pyridine / 5 h

With pyridine; 2,3,5-trimethyl-pyridine; hydrogenchloride; molecular sieve; hydrogen sulfide; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; water; triethylamine; N,N-dimethyl-formamide;