C₆₀H₇₅N₇O₉

Base Information

• Chemical Name: C₆₀H₇₅N₇O₉
• CAS No.: 144582-39-8
• Molecular Formula: C₆₀H₇₅N₇O₉
• Molecular Weight: 1038.3
• Mol file: 144582-39-8.mol

Synonyms:C₆₀H₇₅N₇O₉

Chemical Property of C₆₀H₇₅N₇O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₇₅N₇O₉

There total 20 articles about C₆₀H₇₅N₇O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bis-(3-bromopropyl)-benzene (19417-59-5) → C60H75N7O9 (144582-39-8)

Guidance literature:

Multi-step reaction with 16 steps

1: 1) NaOEt, 2) aq. KOH / 1) EtOH

2: dimethylformamide / Heating

3: TsOH / toluene

4: NaNO₂, CF₃CO₂H

5: aq. KOH

6: SOCl₂ / Heating

7: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

8: B₂H₆ / tetrahydrofuran

9: H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

10: PhCH₂ONa / 100 °C / 12 Torr

11: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

12: dimethylformamide / Heating

13: POCl₃ / CH₂Cl₂

14: cyclohexylamine / toluene / Heating

15: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

16: acetic acid / 70 °C

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; cyclohexylamine; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

[1,4-phenylene]-bis(3-hydroxypropane) (19417-58-4) → C60H75N7O9 (144582-39-8)

Guidance literature:

Multi-step reaction with 17 steps

1: HBr

2: 1) NaOEt, 2) aq. KOH / 1) EtOH

3: dimethylformamide / Heating

4: TsOH / toluene

5: NaNO₂, CF₃CO₂H

6: aq. KOH

7: SOCl₂ / Heating

8: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

9: B₂H₆ / tetrahydrofuran

10: H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

11: PhCH₂ONa / 100 °C / 12 Torr

12: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

13: dimethylformamide / Heating

14: POCl₃ / CH₂Cl₂

15: cyclohexylamine / toluene / Heating

16: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

17: acetic acid / 70 °C

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen bromide; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; cyclohexylamine; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

3,3'-(1,4-phenylene)dipropanoic acid (4251-21-2) → C60H75N7O9 (144582-39-8)

Guidance literature:

Multi-step reaction with 19 steps

1: 1) SOCl₂, 2) NEt₃

2: B₂H₆

3: HBr

4: 1) NaOEt, 2) aq. KOH / 1) EtOH

5: dimethylformamide / Heating

6: TsOH / toluene

7: NaNO₂, CF₃CO₂H

8: aq. KOH

9: SOCl₂ / Heating

10: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

11: B₂H₆ / tetrahydrofuran

12: H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

13: PhCH₂ONa / 100 °C / 12 Torr

14: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

15: dimethylformamide / Heating

16: POCl₃ / CH₂Cl₂

17: cyclohexylamine / toluene / Heating

18: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

19: acetic acid / 70 °C

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen bromide; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; cyclohexylamine; toluene-4-sulfonic acid; triethylamine; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

upstream raw materials:

[1,4-phenylene]-bis(3-hydroxypropane)

1,4-bis-(3-bromopropyl)-benzene

3,3'-(1,4-phenylene)dipropanoic acid

3-[4-(2-ethoxycarbonyl-ethyl)-phenyl]-propionic acid ethyl ester

Downstream raw materials:

C₄₈H₆₁N₅O₇