methyl 2-(6'-phenyltetracyclo<5,4,2,0^3,13,0^10,12>trideca-4',8'-dien-11'-yl)acetate

Base Information

• Chemical Name: methyl 2-(6'-phenyltetracyclo<5,4,2,0^3,13,0^10,12>trideca-4',8'-dien-11'-yl)acetate
• CAS No.: 74635-24-8
• Molecular Formula: C₂₂H₂₄O₂
• Molecular Weight: 320.431

Synonyms:methyl 2-(6'-phenyltetracyclo<5,4,2,0^3,13,0^10,12>trideca-4',8'-dien-11'-yl)acetate

Chemical Property of methyl 2-(6'-phenyltetracyclo<5,4,2,0^3,13,0^10,12>trideca-4',8'-dien-11'-yl)acetate

Chemical Property:

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Technology Process of methyl 2-(6'-phenyltetracyclo<5,4,2,0^3,13,0^10,12>trideca-4',8'-dien-11'-yl)acetate

There total 4 articles about methyl 2-(6'-phenyltetracyclo<5,4,2,0^3,13,0^10,12>trideca-4',8'-dien-11'-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

(3E,9E,12E,14E)-15-Phenyl-pentadeca-3,9,12,14-tetraene-5,7-diynoic acid methyl ester (82706-76-1) → methyl 2-(6'-phenyltetracyclo<5,4,2,03,13,010,12>trideca-4',8'-dien-11'-yl)acetate (74635-24-8) + endiandric acid E ethyl ester (82768-65-8) + endiandric acid D methyl ester (82706-78-3)

Guidance literature:

With quinoline; hydrogen; Lindlar's catalyst; at 25 ℃;

DOI:10.1021/ja00384a080

Reference yield:

(3E,9E,12E,14E)-15-Phenyl-pentadeca-3,9,12,14-tetraene-5,7-diynoic acid methyl ester (82706-76-1) → methyl 2-(6'-phenyltetracyclo<5,4,2,03,13,010,12>trideca-4',8'-dien-11'-yl)acetate (74635-24-8)

Guidance literature:

With quinoline; hydrogen; Lindlar's catalyst; Yield given. Multistep reaction; 1.) 25 deg C, 2.) toluene, 100 deg C;

DOI:10.1021/ja00384a080

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + (±)-endiandric acid A (74591-03-0) → methyl 2-(6'-phenyltetracyclo<5,4,2,03,13,010,12>trideca-4',8'-dien-11'-yl)acetate (74635-24-8)

Guidance literature:

DOI:10.1039/c39800000162

upstream raw materials:

diazomethane

(±)-endiandric acid A

methanol

(3E,9E,12E,14E)-15-Phenyl-pentadeca-3,9,12,14-tetraene-5,7-diynoic acid methyl ester

Downstream raw materials:

(±)-endiandric acid A

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