CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

Base Information

• Chemical Name: CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆
• CAS No.: 1073183-67-1
• Molecular Formula: C₁₂H₁₄N₃O₂*F₆P
• Molecular Weight: 377.226
• Mol file: 1073183-67-1.mol

Synonyms:CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

Chemical Property of CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

There total 4 articles about CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate (1073183-65-9) → CH3N2C3H3CH2C6H3(OH)CHNOH(1+)*PF6(1-)=(CH3NC3H3NCH2C6H3(OH)CHNOH)PF6 (1073183-67-1)

Guidance literature:

1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate; With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 25 - 30 ℃;

With hydrogenchloride; In ethanol; water;

Reference yield:

5-(chloromethyl)salicylaldehyde (23731-06-8) → CH3N2C3H3CH2C6H3(OH)CHNOH(1+)*PF6(1-)=(CH3NC3H3NCH2C6H3(OH)CHNOH)PF6 (1073183-67-1)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene / 3 h / 20 °C / Inert atmosphere

2: hexafluorophosphoric acid / water / 4 h / 20 °C / Cooling with ice

3: hydroxylamine hydrochloride; sodium hydroxide / 1 h / 20 °C

With hexafluorophosphoric acid; hydroxylamine hydrochloride; sodium hydroxide; In water; toluene;

DOI:10.1139/v11-106

Reference yield:

3-(3-formyl-4-hydroxybenzyl)-1-methyl-1H-imidazole-3-ium chloride (1073183-74-0) → CH3N2C3H3CH2C6H3(OH)CHNOH(1+)*PF6(1-)=(CH3NC3H3NCH2C6H3(OH)CHNOH)PF6 (1073183-67-1)

Guidance literature:

Multi-step reaction with 2 steps

1: hexafluorophosphoric acid / water / 4 h / 20 °C / Cooling with ice

2: hydroxylamine hydrochloride; sodium hydroxide / 1 h / 20 °C

With hexafluorophosphoric acid; hydroxylamine hydrochloride; sodium hydroxide; In water;

DOI:10.1139/v11-106

upstream raw materials:

1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate

3-(3-formyl-4-hydroxybenzyl)-1-methyl-1H-imidazole-3-ium chloride

5-(chloromethyl)salicylaldehyde

salicylaldehyde