CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

Base Information

Chemical Name:CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆
CAS No.:1073183-67-1
Molecular Formula:C₁₂H₁₄N₃O₂*F₆P
Molecular Weight:377.226
Hs Code.:

CH<sub>3</sub>N<sub>2</sub>C<sub>3</sub>H<sub>3</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>3</sub>(OH)CHNOH<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NCH<sub>2</sub>C<sub>6</sub>H<sub>3</sub>(OH)CHNOH)PF<sub>6</sub>

Synonyms:CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

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Chemical Property of CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

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Technology Process of CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

There total 4 articles about CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1073183-65-9
1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate

: 1073183-67-1
CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

Guidance literature:: 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate; With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 25 - 30 ℃;

With hydrogenchloride; In ethanol; water;

Reference yield:

: 23731-06-8
5-(chloromethyl)salicylaldehyde

: 1073183-67-1
CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 3 h / 20 °C / Inert atmosphere

2: hexafluorophosphoric acid / water / 4 h / 20 °C / Cooling with ice

3: hydroxylamine hydrochloride; sodium hydroxide / 1 h / 20 °C

With hexafluorophosphoric acid; hydroxylamine hydrochloride; sodium hydroxide; In water; toluene;
DOI:10.1139/v11-106

Reference yield:

: 1073183-74-0
3-(3-formyl-4-hydroxybenzyl)-1-methyl-1H-imidazole-3-ium chloride

: 1073183-67-1
CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆

Guidance literature:: Multi-step reaction with 2 steps

1: hexafluorophosphoric acid / water / 4 h / 20 °C / Cooling with ice

2: hydroxylamine hydrochloride; sodium hydroxide / 1 h / 20 °C

With hexafluorophosphoric acid; hydroxylamine hydrochloride; sodium hydroxide; In water;
DOI:10.1139/v11-106