Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester

Base Information

• Chemical Name: Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester
• CAS No.: 261527-22-4
• Molecular Formula: C₁₅H₂₁NO₂S
• Molecular Weight: 279.403

Synonyms:Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester

Chemical Property of Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester

Chemical Property:

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Technology Process of Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester

There total 1 articles about Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

5-tert-Butyl-4-hydroxy-2-methylbenzaldehyde (16805-16-6) + N,N-Dimethylthiocarbamoyl chloride (16420-13-6) → Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester (261527-22-4)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; at 20 ℃; pH=12 - 12.3;

DOI:10.1080/00304940009355949

Reference yield: 50.0%

Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester (261527-22-4) → Dimethylthiocarbamic acid S-(2-tert-butyl-4-formyl-5-methylphenyl) ester (261527-23-5)

Guidance literature:

With Tetraethylene glycol dimethyl ether; at 250 ℃; for 2h;

DOI:10.1080/00304940009355949

Reference yield:

tetraethylene glycol dimethyl ether + Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester (261527-22-4) → Dimethylthiocarbamic acid S-(2-tert-butyl-4-formyl-5-methylphenyl) ester (261527-23-5)

Guidance literature:

In methanol; water;

upstream raw materials:

5-tert-Butyl-4-hydroxy-2-methylbenzaldehyde

N,N-Dimethylthiocarbamoyl chloride

Downstream raw materials:

Dimethylthiocarbamic acid S-(2-tert-butyl-4-formyl-5-methylphenyl) ester

2-tert-Butyl-4-hydroxymethyl-5-methylthiophenol

toluene-4-thiosulfonic acid S-(2-tert-butyl-4-hydroxymethyl-5-methyl-phenyl) ester

Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

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