Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

Base Information

Chemical Name:Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester
CAS No.:261527-24-6
Molecular Formula:C₁₅H₂₃NO₂S
Molecular Weight:281.419
Hs Code.:

Synonyms:Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

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Chemical Property of Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

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Technology Process of Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

There total 3 articles about Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 261527-23-5
Dimethylthiocarbamic acid S-(2-tert-butyl-4-formyl-5-methylphenyl) ester

: 261527-24-6
Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

Guidance literature:: With lithium borohydride; In tetrahydrofuran; for 1.5h;
DOI:10.1080/00304940009355949

Reference yield:

: 16805-16-6
5-tert-Butyl-4-hydroxy-2-methylbenzaldehyde

: 261527-24-6
Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / aq. KOH / tetrahydrofuran / 20 °C / pH 12 - 12.3

2: 50 percent / tetraethylene glycol dimethyl ether / 2 h / 250 °C

3: 5.6 g / LiBH₄ / tetrahydrofuran / 1.5 h

With potassium hydroxide; lithium borohydride; Tetraethylene glycol dimethyl ether; In tetrahydrofuran; 2: Newman-Kwart rearrangement;
DOI:10.1080/00304940009355949

Reference yield:

: 261527-22-4
Dimethylthiocarbamic acid O-(2-tert-butyl-4-formyl-5-methylphenyl) ester

: 261527-24-6
Dimethylthiocarbamic acid S-(2-tert-butyl-4-hydroxymethyl-5-methylphenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / tetraethylene glycol dimethyl ether / 2 h / 250 °C

2: 5.6 g / LiBH₄ / tetrahydrofuran / 1.5 h

With lithium borohydride; Tetraethylene glycol dimethyl ether; In tetrahydrofuran; 1: Newman-Kwart rearrangement;
DOI:10.1080/00304940009355949