(1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate

Base Information

Chemical Name:(1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate
CAS No.:1573114-47-2
Molecular Formula:C₂₀H₁₈F₃NO₂
Molecular Weight:361.364
Hs Code.:

Synonyms:(1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate

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Technology Process of (1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate

There total 2 articles about (1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 402-50-6
1-trifluoromethyl-4-vinyl-benzene

: 762242-53-5
1-phenylvinyl N,N-dimethylcarbamate

: 1573114-47-2
(1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; In 1,4-dioxane; at 100 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ol500258q

Reference yield:

: 98-86-2
acetophenone

: 1573114-47-2
(1Z,3E)-1-phenyl-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-yldimethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 20 °C

2.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; copper diacetate / 1,4-dioxane / 16 h / 100 °C / Schlenk technique; Inert atmosphere

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; sodium hydride; In 1,4-dioxane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ol500258q