ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride

Base Information

Chemical Name:ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride
CAS No.:82128-91-4
Molecular Formula:C₁₁H₁₄N₂O₅*ClH
Molecular Weight:290.703
Hs Code.:

Synonyms:ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride

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Chemical Property of ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride

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Technology Process of ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride

There total 3 articles about ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 64-17-5
ethanol

: 82128-90-3
2-(2-methoxy-5-nitrophenyl)-2-trimethylsiloxyethanenitrile

: 82128-91-4
ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride

Guidance literature:: With hydrogenchloride; at 5 ℃; for 16h;
DOI:10.1021/jm00155a030

Reference yield:

: 25016-02-8
2-methoxy-5-nitrobenzaldehyde

: 82128-91-4
ethyl 1-hydroxy-1-(2-methoxy-5-nitrophenyl)methanecarboximidate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: ZnI₂ / CH₂Cl₂ / 65 h / Ambient temperature

2: 89 percent / HCl / 16 h / 5 °C

With hydrogenchloride; zinc(II) iodide; In dichloromethane;
DOI:10.1021/jm00155a030