4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

Base Information

• Chemical Name: 4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile
• CAS No.: 1289514-30-2
• Molecular Formula: C₂₄H₂₂N₂O₂S
• Molecular Weight: 402.517

Synonyms:4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

Chemical Property of 4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

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Technology Process of 4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

There total 1 articles about 4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-hydroxy-3-ethoxybenzaldehyde (121-32-4) + 6-Acetyl-1,2,3,4-tetrahydronaphthalene (774-55-0) + Cyanothioacetamide (7357-70-2) → 4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile (1289514-30-2)

Guidance literature:

With ammonium acetate; In butan-1-ol; for 3h; Reflux;

DOI:10.3390/molecules16043410

Reference yield: 79.0%

4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile (1289514-30-2) + 1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside (3068-32-4) → 4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosylthio)pyridine-3-carbonitrile (1384872-98-3)

Guidance literature:

With potassium hydroxide; In ethanol; water; acetone; at 20 ℃;

DOI:10.3390/molecules17044717

Reference yield: 68.0%

4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile (1289514-30-2) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → 4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)pyridine-3-carbonitrile (1384872-96-1)

Guidance literature:

With potassium hydroxide; In ethanol; water; acetone; at 20 ℃;

DOI:10.3390/molecules17044717

upstream raw materials:

4-hydroxy-3-ethoxybenzaldehyde

6-Acetyl-1,2,3,4-tetrahydronaphthalene

Cyanothioacetamide

Downstream raw materials:

4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)pyridine-3-carbonitrile

4-(3-ethoxy-4-hydroxyphenyl)-6-(1,2,3,4-tetrahydronaphthalen-6-yl)-2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosylthio)pyridine-3-carbonitrile

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