15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

Base Information

Chemical Name:15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene
CAS No.:106967-41-3
Molecular Formula:C₃₄H₃₉BrN₄O₆S₃
Molecular Weight:775.809
Hs Code.:

Synonyms:15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

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Chemical Property of 15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

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Technology Process of 15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

There total 2 articles about 15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 106967-42-4
4-bromo-2,6-bis(bromomethyl)pyridine

: 56479-75-5
N,N',N''-tritosyl-4-aza-1,7-heptandiamine disodium salt

: 106967-41-3
15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

Guidance literature:: In N,N-dimethyl-formamide; at 75 ℃; for 2h;

Reference yield:

: 106967-41-3
15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

Guidance literature:

Reference yield:

: 106967-41-3
15-bromo-3,7,11-tritosyl-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

: 128184-02-1
15-(phenylethynyl)-3,7,11-tris(carboxymethyl)-3,7,11,17-tetraazabicyclo<11.3.1>heptadeca-1(17),13,15-triene

Guidance literature:: Multi-step reaction with 4 steps

1: conc. sulfuric acid / 8 h / 105 - 110 °C

2: 39 percent / potassium carbonate / acetonitrile / 24 h / Ambient temperature

3: 63 percent / triethylamine / bis(triphenylphosphine)palladium(II) chloride, copper(I) iodide / tetrahydrofuran / 24 h / 45 °C

4: 100 percent / trifluoroacetic acid / 1.5 h / Ambient temperature

With sulfuric acid; potassium carbonate; triethylamine; trifluoroacetic acid; copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; In tetrahydrofuran; acetonitrile;