(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

Base Information

Chemical Name:(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester
CAS No.:223930-13-0
Molecular Formula:C₂₈H₂₈F₁₇N₃O₇
Molecular Weight:841.519
Hs Code.:

(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

Synonyms:(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

Suppliers and Price of (3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

There total 3 articles about (3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 142010-50-2
3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl isocyanate

: 223930-07-2
N-(2,2-dimethyl-5-hydroxymethyl-[1,3]dioxan-5-yl)-N^α-(benzyloxycarbonyl)glycinamide

: 223930-13-0
(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; Heating;
DOI:10.1021/jo982343+

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 223930-13-0
(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / EEDQ / ethanol / Heating

2: 85 percent / p-TsOH / acetonitrile / 20 °C

3: 90 percent / DABCO / toluene / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; toluene-4-sulfonic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In ethanol; toluene; acetonitrile; 1: Condensation / 2: Condensation / 3: Addition;
DOI:10.1021/jo982343+

Reference yield:

: 91202-74-3
N-<2-hydroxy-1,1-bis(hydroxymethyl)ethyl>-N^α-(benzyloxycarbonyl)glycinamide

: 223930-13-0
(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-carbamic acid 5-(2-benzyloxycarbonylamino-acetylamino)-2,2-dimethyl-[1,3]dioxan-5-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / p-TsOH / acetonitrile / 20 °C

2: 90 percent / DABCO / toluene / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; toluene-4-sulfonic acid; In toluene; acetonitrile; 1: Condensation / 2: Addition;
DOI:10.1021/jo982343+