(3,5-Dimethoxybenzyl)methylamine

Base Information

• Chemical Name: (3,5-Dimethoxybenzyl)methylamine
• CAS No.: 77775-71-4
• Molecular Formula: C10H15NO2
• Molecular Weight: 181.235
• Hs Code.: 2922299090
• European Community (EC) Number: 854-716-0
• Mol file: 77775-71-4.mol

Synonyms:(3,5-Dimethoxybenzyl)methylamine;77775-71-4;1-(3,5-dimethoxyphenyl)-N-methylmethanamine;[(3,5-dimethoxyphenyl)methyl](methyl)amine;3,5-Dimethoxy-N-methylbenzylamine;MFCD05864733;SCHEMBL681502;CDA77571;AKOS000212312;DS-9224;(3 pound not5-Dimethoxybenzyl)methylamine;SY096655;CS-0029514;FT-0704080;EN300-32328;N-Hydroxy-[1,1'-biphenyl]-4-carboximidamide;A865158;(3,5-Dimethoxyphenyl)-N-methylmethanamine, AldrichCPR;Z102767670

Chemical Property of (3,5-Dimethoxybenzyl)methylamine

Chemical Property:

• Vapor Pressure: 0.006mmHg at 25°C
• Refractive Index: 1.501
• Boiling Point: 272.741 °C at 760 mmHg
• PKA: 9.37±0.10(Predicted)
• Flash Point: 108.61 °C
• PSA: 30.49000
• Density: 1.012 g/cm³
• LogP: 1.81410
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 181.110278721
• Heavy Atom Count: 13
• Complexity: 129

Purity/Quality:

97% ^*data from raw suppliers

(3,5-Dimethoxybenzyl)methylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNCC1=CC(=CC(=C1)OC)OC

Technology Process of (3,5-Dimethoxybenzyl)methylamine

There total 1 articles about (3,5-Dimethoxybenzyl)methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethoxybenzaldehdye (7311-34-4) + methylamine (74-89-5) → N-methyl-3,5-dimethoxybenzylamine (77775-71-4)

Guidance literature:

With sodium tetrahydroborate; Yield given. Multistep reaction; 1) r.t., overnight, EtOH-water, 2) 1 h, EtOH-water;

DOI:10.1248/cpb.29.128

Reference yield: 99.0%

ethyl 6-benzyl-4-hydroxy-1-methyl-2-oxo-1,2,5,6,7,8-hexahydro1,6-naphthyridine-3-carboxylate + N-methyl-3,5-dimethoxybenzylamine (77775-71-4) → 6-benzyl-N-(3,5-dimethoxybenzyl)-4-hydroxy-N,1-dimethyl-2- oxo-1,2,5,6,7,8-hexahydro-1,6-naphthyridine-3-carboxamide

Guidance literature:

In toluene; at 110 ℃; for 15h;

DOI:10.1016/j.bmc.2020.115376

Reference yield: 85.0%

ethyl 4-hydroxy-1-methyl-2-oxo-1,2-dihydroquinoline-3-carboxylate (57513-54-9) + N-methyl-3,5-dimethoxybenzylamine (77775-71-4) → N-(3,5-dimethoxybenzyl)-4-hydroxy-N,1-dimethyl-2-oxo-1,2- dihydroquinoline-3-carboxamide

Guidance literature:

In toluene; at 120 ℃; for 12h;

DOI:10.1016/j.bmc.2020.115376

upstream raw materials:

3,5-dimethoxybenzaldehdye

methylamine

Downstream raw materials:

(3,5-Dimethoxy-cyclohexa-2,5-dienylmethyl)-methyl-amine

C₃₆H₄₈FN₃O₈

2-(4-Methyl-piperazin-1-yl)-5-o-tolyl-pyrimidine-4-carboxylic acid (3,5-dimethoxy-benzyl)-methyl-amide

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