bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine

Base Information

Chemical Name:bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine
CAS No.:1442637-86-6
Molecular Formula:C₂₇H₃₁N₃S₂
Molecular Weight:461.695
Hs Code.:

Synonyms:bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine

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Technology Process of bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine

There total 3 articles about bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 13616-82-5
2,4-dimethyl-thiophenol

: 20028-40-4
C-(1-methyl-1H-benzoimidazol-2-yl)-methylamine

: 1442637-86-6
bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine

Guidance literature:: In toluene; at 90 ℃; for 7h; Molecular sieve;
DOI:10.1002/chem.201203498

Reference yield:

: 1442637-90-2
C₁₅H₂₁N₆⁽¹⁺⁾*Cl^(1-)

: 1442637-86-6
bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol; water / 24 h

2: toluene / 7 h / 90 °C / Molecular sieve

With hydrogenchloride; In ethanol; water; toluene;
DOI:10.1002/chem.201203498

Reference yield:

: 4760-35-4
2-chloromethyl-1-methyl-1H-benzimidazole

: 1442637-86-6
bis(2,4-dimethylphenylthiomethyl)-(1-methylbenzimidazol-2-ylmethyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform / 24 h / 60 °C

2: hydrogenchloride / ethanol; water / 24 h

3: toluene / 7 h / 90 °C / Molecular sieve

With hydrogenchloride; In ethanol; chloroform; water; toluene;
DOI:10.1002/chem.201203498