methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside
CAS No.:1032716-06-5
Molecular Formula:C₃₁H₃₄O₉
Molecular Weight:550.606
Hs Code.:

Synonyms:methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside

There total 1 articles about methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 946512-97-6
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

: 1032716-06-5
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside

Guidance literature:: With lithium hydroxide; In methanol; heating;
DOI:10.1002/chem.200701151

Reference yield: 89.0%

: 1032716-06-5
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside

: 1124225-72-4
(3aR,4R,5S,6R,7aR)-4,5-bis(benzyloxy)-6-benzyloxymethyl-2-oxohexahydrofuro[2,3-b]pyran

Guidance literature:: With acetic acid; In toluene; at 110 ℃; for 1h; pH=3 - 4; Inert atmosphere;
DOI:10.1016/j.tet.2011.01.069

Reference yield:

: 1032716-06-5
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(dicarboxy)methyl]-β-D-glucopyranoside

: 1124226-02-3
C₂₉H₃₁N₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / toluene / 1 h / 110 °C / pH 3 - 4 / Inert atmosphere

2.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate / dichloromethane / Inert atmosphere

With calcium sulfate; sodium hydrogencarbonate; acetic acid; scandium tris(trifluoromethanesulfonate); In dichloromethane; toluene;
DOI:10.1016/j.tet.2011.01.069