methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside
CAS No.:946512-97-6
Molecular Formula:C₃₃H₃₈O₉
Molecular Weight:578.659
Hs Code.:

Synonyms:methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

There total 3 articles about methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 108-59-8
malonic acid dimethyl ester

: 946512-97-6
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

: methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-α-Dmannopyranoside

Guidance literature:: With ammonium cerium(IV) nitrate; sodium hydrogencarbonate; In methanol; at 0 ℃; for 0.5h;
DOI:10.1039/b703358c

Reference yield: 78.0%

: 67-56-1
methanol

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 108-59-8
malonic acid dimethyl ester

: 946512-97-6
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

: methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-α-Dmannopyranoside

Guidance literature:: With ammonium cerium(IV) nitrate; sodium hydrogencarbonate; at 0 ℃;
DOI:10.1002/chem.200701151

Reference yield:

: 67-56-1
methanol

: 1334529-20-2
C₃₁H₃₂O₈

: 946512-97-6
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-glucopyranoside

: C₃₃H₃₈O₉

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 4h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c1cc13425f