[(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine

Base Information

Chemical Name:[(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine
CAS No.:79761-10-7
Molecular Formula:C₃₁H₃₄N₂O₇S
Molecular Weight:578.686
Hs Code.:

Synonyms:[(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine

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Chemical Property of [(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine

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Technology Process of [(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine

There total 4 articles about [(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 3054-01-1,25988-62-9
S-benzyl-L-cysteine

: (S)-2-Benzyloxycarbonylamino-6-isobutoxycarbonyloxy-6-oxo-hexanoic acid benzyl ester

: 79761-10-7
[(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine

Guidance literature:: With triethylamine; In water; for 0.833333h; Ambient temperature;
DOI:10.1039/P19810002253

Reference yield:

: 24325-14-2
(2S)-2-[(phenylmethoxy)carbonyl]aminoadipic acid

: 79761-10-7
[(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) caesium carbonate / 1.) methanol, water, 2.) DMF, 50 deg C, 30 min

2: triethylamine, isobutyl chloroformate / tetrahydrofuran / 0.75 h / -15 °C

3: 69 percent / triethylamine / H₂O / 0.83 h / Ambient temperature

With caesium carbonate; triethylamine; isobutyl chloroformate; In tetrahydrofuran; water;
DOI:10.1039/P19810002253

Reference yield:

: 100-39-0
benzyl bromide

: 79761-10-7
[(N-benzyloxycarbonyl)-(α-benzyl)-δ-(L-α-aminoadipoyl)]-S-benzyl-L-cysteine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) caesium carbonate / 1.) methanol, water, 2.) DMF, 50 deg C, 30 min

2: triethylamine, isobutyl chloroformate / tetrahydrofuran / 0.75 h / -15 °C

3: 69 percent / triethylamine / H₂O / 0.83 h / Ambient temperature

With caesium carbonate; triethylamine; isobutyl chloroformate; In tetrahydrofuran; water;
DOI:10.1039/P19810002253